Multispectral Analysis 1 Questions

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Question 1

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

IR Spec

C-13 NMR

Proton NMR


Question 2

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

IR Spec

C-13 NMR

Proton NMR


Question 3

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

The molecular ion peak is at 144.

Chemical Analysis

The compound is reacted against acidified potassium dichromate and no reaction occurs. The compound is reacted against bromine water and no reaction occurred.

C-13 NMR

Proton NMR


Question 4

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

IR-Spec

C-13 NMR

Proton NMR


Question 5

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

Chemical Analysis

  • The compound is reacted with sodium carbonate and there is no reaction.
  • When reacted with sulfuric acid, and then the sulfuric acid removed, the product is still acidic.

The compound is reacted with dichromate and (separately) Tollens reagent. Neither test produced a positive result.

C-13 NMR

Proton NMR


Question 1

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

IR Spec

C-13 NMR

Proton NMR

Answer


Question 2

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

IR Spec

C-13 NMR

Proton NMR

Answer


Question 3

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

The molecular ion peak is at 144.

Chemical Analysis

The compound is reacted against acidified potassium dichromate and no reaction occurs. The compound is reacted against bromine water and no reaction occurred.

C-13 NMR

Proton NMR

Answer


Question 4

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

IR-Spec

C-13 NMR

Proton NMR

Answer


Question 5

A substance is analysed using a variety of techniques, the results of which are outlined below. Use the information provided to determine the structure of the substance.

Mass Spec

Chemical Analysis

  • The compound is reacted with sodium carbonate and there is no reaction.
  • When reacted with sulfuric acid, and then the sulfuric acid removed, the product is still acidic.

The compound is reacted with dichromate and (separately) Tollens reagent. Neither test produced a positive result.

C-13 NMR

Proton NMR

Answer